Drexel Nanotechnology InstituteMaterials and Nanotechnology ConsortiumAn NSF Integrated Graduate Education and Research Traineeship in Nanoscale Science & EngineeringResearch Experience for Teachers in the Area of NanotechnologyMaterials Science and EngineeringCollege of Engineering

• Raman Micro Spectrometer Renishaw 1000
• UV Raman Microspectrometer
• FTIR Spectroscope with Microscope (Digilab, UMA 600)
• Surface Area and Pore Size Analyzer (Quantachrome, Autosorb-1)

• Tube Furnaces
 

Raman Micro Spectrometer (Renishaw 1000)

Raman Spectroscopy

Important Features
• Ar ion laser, 514.5 nm
• He-Ne laser, 633 nm
• Semiconductor diode laser, 785 nm
• -70° Centigrade Peltier cooled CCD detector
• XYZ motorized mapping stage
• 100 cm-1 cutoff notch filter
• Magnification up to 1000x (x5, x20, x50, x100 objectives)
• Grams 32 spectral analysis software, and geological spectra database
• 8000 cm-1 extended scanning range
• 1800 l/mm and 1200 l/mm gratings
•Direct Raman imaging through dielectric filters
• Videocamera and image capture card

 

* Tutorial
* For more information, contact Dr. Zhorro Nikolov
* Sign out time on the Raman
* Billing Rate: University Internal($25/hour unassisted, $45/hour assisted), University External ($30/hour unassisted, $55/hour assisted) Unassisted work is possible only after a training course. Equipment Use Form.



UV Raman Microspectrometer

Raman Spectroscopy

Important Features
• Magnifying and imaging capabilities
• Motorized XYZ stages
• Heating/Freezing stages
•  Choice of excitation wavelength (UV, Visible, near IR, Circular Polarized light)
• 'Easy Confocal' microscopy
• Rapid, non-destructive
• Easy or no sample preparation (solids, liquids, gases)
• High Spectral/Spatial resolution

 

* For more information, contact Dr. Zhorro Nikolov
* Billing Rate: University Internal ($40/hour unassisted, $60/hour assisted), University External ($60/hour unassisted, $85/hour assisted). Unassisted work is possible only after a training course. Equipment Use Form.



FTIR Spectroscope with Microscope (Digilab, UMA 600)

Raman Spectroscopy

Important Features
• The advanced optical design eliminates stray light and the need for redundant aperturing
• Samples can be viewed by both binocular and video modes
• Infinity corrected, all reflecting optics without the need for dichroics provides the ultimate in detectability and throughput
• Dual detector capability equips the microscope with two single point detectors, an array and a single point detector or dual focal plane arrays, to minimize the "down time" of detector changes
• Zoom capability in both visible and IR gives the flexibility to use higher magnification if necessary without physically changing the objective
• A motorized aperture gives precise control from either the computer or the microscope and enhances the ease of use
• Auto focus in both the infrared for sample analysis and in the visible for video camera assures that the picture you see or the data you acquire are optimal
• Automated multi point analysis (AMPA™) allows unattended analysis of many points on the same samples or many samples on the sample holder

* For more information, contact Dr. Zhorro Nikolov
* Billing Rate: University Internal ($25/hour unassisted, $45/hour assisted), University External ($30/hour unassisted, $55/hour assisted). Unassisted work is possible only after a training course. Equipment Use Form.



Surface Area and Pore Size Analyzer (Quantachrome, Autosorb -1)

Raman Spectroscopy

Important Features
• A fully automated analyzer for surface area and pore size measurements
• Offers simultaneous analysis and sample preparation
• Low maintenance, vacuum volumetric system with stainless steel manifold construction
• Speed and precision ensured by MaxiDose™, a proprietary dosing algorithm
• High sensitivity ensured by multiple pressure transducers, minimum void volume and accurate coolant level control
• Operates with any non-corrosive adsorbate and a wide variety of coolants, including slurries
• DoseWizard™ learn mode and InitialFill™ for analysis time savings of up to 60 percent

* For more information, contact Mr. John Chmiola
* For more information about Quantachrome, Autosorb-1, please visit here.
* Billing Rate: University Internal ($10/hour unassisted, $30/hour assisted), University External ($50/hour unassisted, $70/hour assisted). Billing Form.


Tube Furnaces

Raman Spectroscopy

Important Features
• Our first furnace is a wound tube furnace with a max temp. of 1200° C with a tube diameter of 25 mm, and a heated length of 250 mm.
• Our second furnace is a high temperature tube furnace with a max temp of 1700° C with tube diameter of 75 mm, and a heated length of 300 mm.
• Our third furnace is a three zone tube furnace with a max temp. of 1200° C with a tube diameter of 75 mm, and a heated length of 700 mm.

 

* For more information, contact Mr. John Chmiola.

 

 

 

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D.N.I | M. C. F. | I.G.E.R.T. | RET-Nnano | Materials Science & Engineering | College of Engineering